原位SEM陶瓷基复合材料拉伸裂纹特征演化规律研究

In-situ SEM study of crack under tensile loading in ceramic matrix composites

  • 摘要: 通过开展2D SiC/SiC复合材料的原位拉伸实验,揭示了外加载荷对材料裂纹特征演化的影响规律。实验结果表明:在单轴拉伸载荷作用下,2D SiC/SiC复合材料的裂纹密度与裂纹宽度均呈现显著的载荷相关性。裂纹密度演化主要受界面脱粘程度影响,当界面脱粘程度较低时,应力传递效率提高,基体容易产生新生裂纹。通过建立描述裂纹密度的威布尔分布模型,和原位试验数据相比,平均绝对误差和和均方根误差分别为0.053和0.077,实现了对裂纹密度-应力关系的准确描述。裂纹宽度扩展则与载荷应力、界面剪切应力密切相关,构建的裂纹宽度-应力模型成功复现了不同载荷阶段裂纹宽度的演化趋势。本研究为陶瓷基复合材料的多尺度损伤表征提供了新的分析方法和理论依据。

     

    Abstract: In-situ tensile experiments of 2D SiC/SiC composites were carried out to reveal the influence law of applied load on the crack evolution characteristics of the materials. The experimental results show that under uniaxial tensile loading, the crack density and crack width of 2D SiC/SiC composites show significant load correlation. The crack density evolution is mainly regulated by the degree of interfacial debonding. When the degree of interfacial debonding is low, the stress transfer efficiency increases and the matrix is prone to nascent cracks. By establishing a Weibull distribution model to describe crack density, the average absolute error and root mean square error are 0.053 and 0.077, respectively, compared with in-situ test data. Accurate description of the relationship between crack density and stress has been achieved. Crack width extension, on the other hand, is closely related to stress and interfacial shear stress. The crack width-stress ontology model was constructed to successfully reproduce the evolution trend of crack width at different loading stages. This study provides a new analytical method and theoretical basis for the multi-scale damage characterization of ceramic matrix composites.

     

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